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Solvent-free synthesis of 6-unsubstituted dihydropyrimidinones using 2-pyrrolidonium bisulphate as efficient catalyst

Heshmatollah Alinezhad, Mahmood Tajbakhsh, Mahboobeh Zare, and Mahbooeh Mousavi

Faculty of Chemistry, University of Mazandaran, University Street, 47416-95447 Babolsar, Iran

 

E-mail: heshmat@umz.ac.ir

Abstract: A one-pot three-component Biginelli-like reaction of enaminones, aldehydes with urea/thiourea in the presence of 2-pyrrolidonium bisulphate as an acidic ionic liquid catalyst for the preparation of 6-unsubstituted dihydropyrimidinones is described. The excellent yield, short reaction time, simple procedure and avoidance of the use of organic solvents are some advantages of this method.

Keywords: 6-unsubstituted dihydropyrimidinone – 2-pyrrolidonium bisuslphate – enaminone – aldehyde – urea/thiourea

Full paper is available at www.springerlink.com.

DOI: 10.1515/chempap-2016-0048

 

Chemical Papers 70 (8) 1126–1130 (2016)

Friday, March 29, 2024

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