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Isothiocyanates and Their Synthetic Producers. XII. Preparation of 3,5-Disubstituted Tetrahydro-1,3,5-thiadiazine-2-thiones Labeled with 14C and 35S

J. Augustín, J. Bernát, Ľ. Drobnica, and P. Kristián

Department of Microbiology and Biochemistry, Slovak Technical University, Bratislava 1

 

Abstract:  The preparation of 3,5-dibenzyltetrahydro-l,3,5-thiadiazine-2-thione-35S by isotopic substitution with 35S is described. Also the preparation of 3-(4-bromophenyl)-5-benzyltetrahydro-l,3,5-thiadiazine-2-thione-35S from 4-bromophenyl isothiocyanate-35S and of 3-benzyl-5-carboxymethyltetrahydro-1,3,5-thiadiazine-2-thione-14C from glycine-14C is described.

Full paper in Portable Document Format: 254a304.pdf

 

Chemical Papers 25 (4) 304–307 (1971)

Thursday, June 17, 2021

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