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Alternative syntheses of methylated sugars. X. Methyl pyranosides of 2-O-methyl-D-glucose

P. Kováč and Ž. Longauerová

Institute of Chemistry, Slovak Academy of Sciences* 809 33 Bratislava

 

Abstract: Methyl 2-O-methyl-a-D-glucopyranoside and methyl 2 -0 -methyl -ß-D-glucopyranoside have been obtained in crystalline condition by methylation of methyl 3-0-benzyl-4,6-0-benzylidene- α,ß-D-glucopyranoside followed by chromatography and removal of the blocking groups in the isolated anomers. Debenzylidenation of methyl 3-0-benzyl-4,6-0-benzylidene-2-0-methyl-α-D-glucopyranoside, methylation and debenzylation afforded methyl 2,4,6-tri-O-methyl-α-D-glucopyranoside

Full paper in Portable Document Format: 273a415.pdf

 

Chemical Papers 27 (3) 415–420 (1973)

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