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Volumetric determination of boric acid in the medium of anhydrous acetic acid

Z. Hladký, M. Čakrt, and J. Berčík

Department of Analytical Chemistry, Slovak Technical University, 880 37 Bratislava

 

Abstract: Boric acid can be determined in the medium of anhydrous acetic acid after its transformation to tetrafluoroboric acid by titrating with the volumetric solution of sodium or potassium acetate, diethylaniline or pyridine in anhy­drous acetic acid. A Potentiometrie or conductometric indication is to be used. The amounts of 1—10 millimoles of boric acid were determined with a relative error which did not exceed 0.3%.

Full paper in Portable Document Format: 344a460.pdf

 

Chemical Papers 34 (4) 460–464 (1980)

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